HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-chloro-5-isocyanato-2,4-dimethoxybenzene → HCID 15907987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-chloro-5-isocyanato-2,4-dimethoxybenzene | HCID 4389804 | — |
| Reactant | HCID 15922851 | HCID 15922851 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15907987 | HCID 15907987 | — |
Reaction Steps
A suspension of N-(4-amino-phenyl)-2-fluoro-benzamide (0.43 g) in acetonitrile (4 mL) is treated with 5-chloro-2,4-dimethoxyphenylisocyanate (0.40 g). The mixture becomes a solution and is allowed to stand for 12 hours. A white solid forms and is collected by filtration (0.79 g). [M+H]444.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462055B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-5b1de3727b94487ebf5f3bba23f1d612 |
| Source note | uspto-grants-2002_10 |