HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11056131, compound → HCID 53756990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11056131 | HCID 11056131 | — |
| Reactant | 2-[4-(Chloromethyl)phenoxy]-N,N-diethylethan-1-amine | HCID 12493691 | — |
| Product | HCID 53756990 | HCID 53756990 | — |
Reaction Steps
2-[4-(2-Diethylaminoethoxy)benzyl]-2-(4-methoxy-benzenesulfonyl)hexanoic acid ethyl ester was prepared according to the general method as outlined in example 12. Starting from 2-(4-methoxy-benzenesulfonyl)hexanoic acid ethyl ester (4 g, 12.7 mmol) and (2-(4-chloromethyl-phenoxy)ethyl]diethylamine (3.38 g, 14 mmol). Yield 8.21 g crude (100%); brown oil; MS: 520.4 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462073B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-ad5cb4844d3d43a6a8870749f117bee4 |
| Source note | uspto-grants-2002_10 |