HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)pentanoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | Ethyl 2-bromovalerate | HCID 79071 | — |
| Product | 2-(4-Methoxy-phenylsulfanyl)pentanoic acid ethyl ester | HCID 54570902 | — |
Reaction Steps
2-(4-Methoxy-phenylsulfanyl)pentanoic acid ethyl ester was prepared according to the general method as outlined in example 9. Starting from ethyl 2-bromovalerate (8.23 g, 39.3 mmol) and 4-methoxythiophenol (5 g, 35.7 mmol), 10.46 g (100%); clear oil; MS: 269 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462073B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-b81780a23054429bb5998ed0226959cf |
| Source note | uspto-grants-2002_10 |