Cyclohexanol → Diphenylacetyl-carbamic acid cyclohexyl ester

HRID 991204Notes

Reaction equation

HRID 991204 reaction equation
[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:19]1([OH:25])[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH:19]1([O:25][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 7966CyclohexanolHCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 69921104Diphenylacetyl-carbamic acid cyclohexyl ester

Procedure

The title compound, white solid, m.p. 117-119° C. and MS: m/e=337.4 (M+H+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and cyclohexanol.

Sources & evidence

ORD record
ord-07189db256854f9290a828096eeedde7
Source dataset
uspto-grants-2002_10
Patent number
US06462198B1

Reaction notes

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