Benzenebutanol → Diphenylacetyl-carbamic acid 4-phenyl-butyl ester

HRID 991205Notes

Reaction equation

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:19]1([CH2:25][CH2:26][CH2:27][CH2:28][OH:29])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:19]1([CH2:25][CH2:26][CH2:27][CH2:28][O:29][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

Reactant 2

HCID 76889Benzenebutanol

HCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 54427908Diphenylacetyl-carbamic acid 4-phenyl-butyl ester

Procedure

The title compound, light yellow solid, m.p.=118° C. and MS: m/e=387.5 (M+H+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and 4-phenyl-butan-1-ol.

Sources & evidence

ORD record: ord-77387b1f3d444d14b3f5afeca76005cf
Source dataset: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06462198B1

Reaction notes

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