Carbamic acid, ethyl ester → HCID 57223634, compound

HRID 991217Notes

Reaction equation

HRID 991217 reaction equation
[F:1][C:2]([F:21])([F:20])[C:3]1[C:16]2[O:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[CH:8]([C:17](Cl)=[O:18])[C:7]=2[CH:6]=[CH:5][CH:4]=1.[CH2:22]([O:24][C:25](=[O:27])[NH2:26])[CH3:23]>>[CH2:22]([O:24][C:25](=[O:27])[NH:26][C:17]([CH:8]1[C:7]2[CH:6]=[CH:5][CH:4]=[C:3]([C:2]([F:21])([F:20])[F:1])[C:16]=2[O:15][C:14]2[C:9]1=[CH:10][CH:11]=[CH:12][CH:13]=2)=[O:18])[CH3:23]

Participants

3

Reactant 2

HCID 5641Carbamic acid, ethyl esterHCID 22661058HCID 22661058, compound

Product 1

HCID 57223634HCID 57223634, compound

Procedure

The title compound, white solid, m.p.=196-198° C., MS: m/e=365 (M+) was prepared in accordance with the general method of example 36 from 4-trifluoromethyl-9H-xanthene-9-carbonyl chloride and carbamic acid ethyl ester.

Sources & evidence

ORD record
ord-2c9214eebbee4786b088e064d226c8c2
Source dataset
uspto-grants-2002_10
Patent number
US06462198B1

Reaction notes

Loading…