Methyl butyrate → Cyclohexane-1,4-dicarbaldehyde

HRID 991397Notes

Reaction equation

HRID 991397 reaction equation
[CH3:1][CH2:2][CH2:3][C:4]([O:6]C)=O>C(CC=O)CC=O>[CH:3]1([CH:4]=[O:6])[CH2:2][CH2:1][CH:3]([CH:4]=[O:6])[CH2:2][CH2:1]1

Participants

3

Reactant 1

HCID 12180Methyl butyrate

Product 1

HCID 10154096Cyclohexane-1,4-dicarbaldehyde

Reagents, catalysts & solvents 1

HCID 3485GlutaraldehydeSolvent

Procedure

The procedure according to Example 17 was repeated, but using the same amount of the polymer obtained from Example 10 instead of the polymer obtained from Example 1; 1,4-cyclohexane dicarboxaldehyde (1.4 g) as a cross-linker instead of glutaric dialdehyde, and methyl 3-methylpropionate (25 ml) as a solvent, to obtain a negative pattern with a resolution of 0.15 μm (FIG. 3).

Sources & evidence

ORD record
ord-17ad5e1751fc420a8e670d8bef2beea1
Source dataset
uspto-grants-2002_10
Patent number
US06465147B1

Reaction notes

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