HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1-propanol → HCID 43393146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | Benzo(b)thiophene-2-carboxylic acid | HCID 95864 | — |
| Product | HCID 43393146 | HCID 43393146 | 52.3% |
Reaction Steps
2-Benzothiophenecarboxylic acid (5.0 g, 28.05 mmol) and 3-amino-1-propanol (2.57 ml, 33.66 mmol) were coupled according to the procedure of Example 22 to provide 3.45 g (52.3% yield) of the desired product as an orange solid. Electrospray Mass Spec: m/z 235.9 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06465508B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-93cef0f5b83249659b1c9e3b767d9cdc |
| Source note | uspto-grants-2002_10 |