HCID 86604207, compound → HCID 9934791, compound

HRID 991761Notes

Reaction equation

HRID 991761 reaction equation
[CH3:1][O:2][C:3]([C:5]12[CH2:14][CH:9]3[CH2:10][CH:11]([CH2:13][C:7]([C:15]([NH:17][C@@H:18]([CH2:26][CH:27]4[CH2:32][CH2:31][CH:30]([O:33][C:34]([N:36]([CH3:38])[CH3:37])=[O:35])[CH2:29][CH2:28]4)[C:19]([O:21]C(C)(C)C)=[O:20])=[O:16])([CH2:8]3)[CH2:6]1)[CH2:12]2)=[O:4]>C(O)=O>[CH3:1][O:2][C:3]([C:5]12[CH2:12][CH:11]3[CH2:10][CH:9]([CH2:8][C:7]([C:15]([NH:17][C@@H:18]([CH2:26][CH:27]4[CH2:28][CH2:29][CH:30]([O:33][C:34]([N:36]([CH3:38])[CH3:37])=[O:35])[CH2:31][CH2:32]4)[C:19]([OH:21])=[O:20])=[O:16])([CH2:13]3)[CH2:6]1)[CH2:14]2)=[O:4]

Participants

3

Reactant 1

HCID 86604207HCID 86604207, compound

Product 1

HCID 9934791HCID 9934791, compound

Reagents, catalysts & solvents 1

HCID 284Formic AcidSolvent

Procedure

The product from Step C was dissolved in formic acid at room temperature and the reaction mixture was stirred overnight. After evaporation of the solvent under reduced pressure, the title compound was isolated as a solid.

Workup

  1. customAfter evaporation of the solvent under reduced pressure

Sources & evidence

ORD record
ord-290cc3fbe5564e28b6d5be5a3a08fa8d
Source dataset
uspto-grants-2002_10
Patent number
US06465513B1

Reaction notes

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