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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 991851Generated: October 26, 2026

Calcium chloride, dihydrate → Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate

https://huagongshe.com/reaction/991851

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCalcium chloride, dihydrateHCID 6093260—
Reactantbicyclo2.2.1heptane-2,3-dicarboxylic acid, disodium saltHCID 21981355—
SolventWaterHCID 962—
ProductCalcium bicyclo(2.2.1)heptane-2,3-dicarboxylateHCID 21981350—

Reaction Conditions

Temperature60 °C

Reaction Steps

To a solution of disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate (22.6 g, 0.1 mols) in water (150 g) was added a solution of calcium chloride dihydrate (14.7 g, 0. 1 mols) in water (100 g). The mixture was stirred at 60° C. for 2 hours. The resulting white precipitate was filtered. The white powdery product was dried and milled (m.p. >300° C.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06465551B1
Source datasetuspto-grants-2002_10
ORD IDord-a6338a05c872476eb95b39e21cb2211f
Source noteuspto-grants-2002_10