Butylamine → HCID 13958330, compound

HRID 991930Notes

Reaction equation

HRID 991930 reaction equation
O[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=[CH:4][C:3]=1[N+:12]([O-:14])=[O:13].[CH2:15]([NH2:19])[CH2:16][CH2:17][CH3:18]>>[CH2:15]([NH:19][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=[CH:4][C:3]=1[N+:12]([O-:14])=[O:13])[CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 8007ButylamineHCID 178526762HCID 178526762, compound

Product 1

HCID 13958330HCID 13958330, compound

Procedure

Using the general method of Example 41, 4-hydroxy-3-nitroquinoline (38.4 g, 0.2 moles) was chlorinated then reacted with n-butylamine (24.7 mL, 0.4 mole) to provide the desired product as a yellow sold.

Sources & evidence

ORD record
ord-18f198e4661a4449a789b4f82beeebe7
Source dataset
uspto-grants-2002_10
Patent number
US06465654B2

Reaction notes

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