HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Fluoroindole → 3-(1,4-Dioxa-spiro[4,5]dec-7-en-8-yl)-6-fluoro-1H-indole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Fluoroindole | HCID 351278 | — |
| Edukt | 3-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-1H-indole | HCID 2763857 | — |
| Produkt | 3-(1,4-Dioxa-spiro[4,5]dec-7-en-8-yl)-6-fluoro-1H-indole | HCID 18414166 | 96,3% |
Reaktionsschritte
This compound was prepared in the manner described for intermediate 1a by replacing indole with 6-fluoroindole (5.14 g, 38 mmol)) to afford 10 g (96.3%) of the title compound as a white solid: mp 196-197° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06465482B2 |
| Quelldatensatz | uspto-grants-2002_10 |
| ORD ID | ord-b67dbcf61572436c89fb0b0958bddcf4 |
| Quellennotiz | uspto-grants-2002_10 |