Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Glycidyl methacrylate | HCID 7837 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21894100 | HCID 21894100 | — |
Reaction Steps
0.035 g sulfuric acid and 0.025 g hydrochinone are dissolved in 64 g water and heated up to 90° C. Within 3 h a total of 50 g glycidylmethacrylate are slowly added to the stirred hot solution. After an additional hour at 90° C. the solution is cooled down to 40° C. The water is removed at about 40 mbar. A clear viscous solution of the monomer glycerol-methacrylate is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06468408B2 |
|---|
| Source dataset | uspto-grants-2002_10 |
|---|
| ORD ID | ord-2279312c3170415cbb4f578a8a5e35b1 |
|---|
| Source note | uspto-grants-2002_10 |
|---|
