HCID 18411537, compound → HCID 18411539, compound

HRID 992209Notes

Reaction equation

HRID 992209 reaction equation
[N:1]1([C:6]2[S:7][CH:8]=[C:9]([CH2:11][OH:12])[N:10]=2)[CH:5]=[N:4][CH:3]=[N:2]1>C(Cl)(Cl)Cl.CO.O=[Mn]=O>[N:1]1([C:6]2[S:7][CH:8]=[C:9]([CH:11]=[O:12])[N:10]=2)[CH:5]=[N:4][CH:3]=[N:2]1

Participants

5

Reactant 1

HCID 18411537HCID 18411537, compound

Product 1

HCID 18411539HCID 18411539, compound

Reagents, catalysts & solvents 3

HCID 14801Manganese dioxideCatalystHCID 887MethanolSolventHCID 6212ChloroformSolvent

Procedure

MnO2 (5.3 g; 60.9 mmol) was added to a solution of (2-[1,2,4]triazol-1-ylthiazole-4-yl)methanol (0.32 g; 2.25 mmol), prepared as described in the above step, in chloroform (15 ml) and methanol (1.5 ml).

Workup

  1. customprepared

Sources & evidence

ORD record
ord-5a74b4aab9874c46b136806df676b8da
Source dataset
uspto-grants-2002_10
Patent number
US06468979B1

Reaction notes

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