HCID 18411543, compound → HCID 18411538, compound

HRID 992211Notes

Reaction equation

HRID 992211 reaction equation
[N:1]1([C:6]2[S:7][CH:8]=[C:9]([CH2:11][OH:12])[N:10]=2)[CH:5]=[CH:4][CH:3]=[N:2]1>C(Cl)(Cl)Cl.O=[Mn]=O>[N:1]1([C:6]2[S:7][CH:8]=[C:9]([CH:11]=[O:12])[N:10]=2)[CH:5]=[CH:4][CH:3]=[N:2]1

Participants

4

Reactant 1

HCID 18411543HCID 18411543, compound

Product 1

HCID 18411538HCID 18411538, compound

Reagents, catalysts & solvents 2

HCID 14801Manganese dioxideCatalystHCID 6212ChloroformSolvent

Procedure

MnO2 (10.8 g; 125 mmol) was added to a solution of (2-pyrazol-1-ylthiazole-4-yl)methanol (1.13 g; 6.24 mmol), prepared as described in the above step, in chloroform (100 ml).

Workup

  1. customprepared

Sources & evidence

ORD record
ord-1ef586128ff64387aed89abb9676870f
Source dataset
uspto-grants-2002_10
Patent number
US06468979B1

Reaction notes

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