HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-amino-3-fluoro-5-nitro-2-(2-toluidino)benzoate → HCID 9823009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-amino-3-fluoro-5-nitro-2-(2-toluidino)benzoate | HCID 22180129 | — |
| Reactant | HCID 22180138 | HCID 22180138 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 9823009 | HCID 9823009 | — |
Reaction Steps
A mixture comprised of methyl 4-amino-3-fluoro-2-(2-methyl-phenylamino)-5-nitrobenzoate (from Step d, Example 1) and iodosobenzenediacetate (1.76 equiv.) in benzene is stirred at ambient temperature for 5 hours. The mixture is concentrated in vacuo and the residue purified by column chromatography to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06469004B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-c58a67db3c674ad5813cad2333122d20 |
| Source note | uspto-grants-2002_10 |