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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 992747Generated: November 1, 2026

Salicylaldehyde → HCID 136048877, compound

https://huagongshe.com/reaction/992747

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSalicylaldehydeHCID 6998—
ReactantHCID 12992022HCID 12992022—
SolventEthanolHCID 702—
SolventTolueneHCID 1140—
ProductHCID 136048877HCID 13604887799.5%

Reaction Steps

0.968 g (2.0 mmol) of (R)-2-amino-1,1-di(2-butoxy-5-t-butylphenyl)-propanol and 0.244 g (2.0 mmol) of salicylaldehyde were dissolved in 20 ml of ethanol and 20 ml of toluene, the solution was heated at reflux for 1 hour. The solvent was distilled off from the reaction mixture and dried to obtain 1.17 g of (R)-N-salicyliden-2-amino-1,1-di(2-butoxy-5-t-butylphenyl)-propanol as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06469198B2
Source datasetuspto-grants-2002_10
ORD IDord-84a95bf76b5e4dd4948ec54e89dd9de3
Source noteuspto-grants-2002_10