HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → HCID 136048877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | HCID 12992022 | HCID 12992022 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 136048877 | HCID 136048877 | 99.5% |
Reaction Steps
0.968 g (2.0 mmol) of (R)-2-amino-1,1-di(2-butoxy-5-t-butylphenyl)-propanol and 0.244 g (2.0 mmol) of salicylaldehyde were dissolved in 20 ml of ethanol and 20 ml of toluene, the solution was heated at reflux for 1 hour. The solvent was distilled off from the reaction mixture and dried to obtain 1.17 g of (R)-N-salicyliden-2-amino-1,1-di(2-butoxy-5-t-butylphenyl)-propanol as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06469198B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-84a95bf76b5e4dd4948ec54e89dd9de3 |
| Source note | uspto-grants-2002_10 |