2,4-Dimethyl-3-pentanone → HCID 18413318, compound

HRID 992776Notes

Reaction equation

HRID 992776 reaction equation
[CH:1]([C:4]([CH:6]([CH3:8])[CH3:7])=[O:5])([CH3:3])[CH3:2].Cl[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH:15]1[CH2:20][CH:19]2[CH2:21][CH:16]1[CH:17]=[CH:18]2>>[CH:1]([C:4]([CH:6]([CH3:8])[CH3:7])([OH:5])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH:15]1[CH2:20][CH:19]2[CH2:21][CH:16]1[CH:17]=[CH:18]2)([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 112712,4-Dimethyl-3-pentanoneHCID 18410366HCID 18410366, compound

Product 1

HCID 18413318HCID 18413318, compoundYield 85%

Procedure

1,1-Diisopropyl-6-(5-norbornen-2-yl)hexanol (yield: 85%) was obtained in the same manner as in Synthesis Example 1, except that diisopropyl ketone and 1-chloro-5-(5-norbornen-2-yl)pentane were used in place of acetone and 1-chloro-4-(5-norbornen-2-yl)butane, respectively.

Sources & evidence

ORD record
ord-061f0baec53f44608b9e014dcc5a504c
Source dataset
uspto-grants-2002_10
Patent number
US06469220B2

Reaction notes

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