HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → 1-Nitro-4-phenoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | Phenolate Sodium | HCID 4445035 | — |
| Product | 1-Nitro-4-phenoxybenzene | HCID 12110 | 98% |
Reaction Steps
The reaction was carried out completely in the same manner as in Example 21, except that p-fluoronitrobenzene was used instead of p-chloronitrobenzene and sodium phenolate was used instead of potassium fluoride in Example 21. Further, the reaction temperature was changed to 80° C. and the reaction time was changed to 3 hours without pursuing the reaction on halfway. Objective 4-phenoxynitrobenzene was produced in the yield of 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06469224B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-b163d26c1bb8485f8e8c80b0e727b98d |
| Source note | uspto-grants-2002_10 |