HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 2-(4-Chloro-2-methoxyphenyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2-(4-Chloro-2-methoxyphenyl)acetonitrile | HCID 22327524 | — |
| Product | 2-(4-Chloro-2-methoxyphenyl)acetic acid | HCID 14675568 | — |
Reaction Steps
141 g of 4-chloro-2-methoxyphenylacetonitrile are reacted with 83.2 g of potassium hydroxide in 280 ml of ethylene glycol. 148 g of solid are obtained (m.p.: 100° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06472419B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-d1ad49578ecc49789247b3cc9681e517 |
| Source note | uspto-grants-2002_10 |