HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Benzylaminosulfonylmethylbenzyl)-nitrobenzene → 4-(4-Benzylaminosulfonylmethylbenzyl)-phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Benzylaminosulfonylmethylbenzyl)-nitrobenzene | HCID 21876751 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | 4-(4-Benzylaminosulfonylmethylbenzyl)-phenylamine | HCID 21876959 | 95.9% |
Reaction Steps
A solution of 4-(4-benzylaminosulfonylmethylbenzyl)-nitrobenzene (44 mg) was dissolved in ethyl acetate and hydrogenated at 40 psi with 10% palladium or carbon catalyst for 2 hours. The mixture was filtered, and the solvent was evaporated to give 4-(4-benzylaminosulfonylmethylbenzyl)-phenylamine (39 mg) as an off- white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06472536B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-8e43017b995d4cd3997ab47244cac982 |
| Source note | uspto-grants-2002_10 |