4-氯-3-甲氧基-2-甲基吡啶 → 4-[O-(4-tert-Butylbenzyl)hydroxylamino]-3-methoxy-2-methylpyridine

HRID 1001

反应方程式

HRID 1001 反应方程式
Cl[C:2]1[CH:7]=[CH:6][N:5]=[C:4]([CH3:8])[C:3]=1[O:9][CH3:10].[C:11]([C:15]1[CH:23]=[CH:22][C:18]([CH2:19][O:20][NH2:21])=[CH:17][CH:16]=1)([CH3:14])([CH3:13])[CH3:12]>>[C:11]([C:15]1[CH:16]=[CH:17][C:18]([CH2:19][O:20][NH:21][C:2]2[CH:7]=[CH:6][N:5]=[C:4]([CH3:8])[C:3]=2[O:9][CH3:10])=[CH:22][CH:23]=1)([CH3:14])([CH3:12])[CH3:13]

参与物

3

反应物 2

HCID 105830464-氯-3-甲氧基-2-甲基吡啶HCID 15279359o-(4-(Tert-butyl)benzyl)hydroxylamine

产物 1

HCID 196940214-[O-(4-tert-Butylbenzyl)hydroxylamino]-3-methoxy-2-methylpyridine收率 80%

实验过程

Prepared analogously to Example 1 from 4-chloro-3-methoxy-2-methylpyridine and O-(4-tert-butylbenzyl)hydroxylamine. Yield: 80%; m.p.: 113° C.

来源与证据

ORD记录
ord-7b37c31faaef4c5bb1868f6f9352f189
来源数据集
uspto-grants-1998_03
专利号
US05723450

关联笔记

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