3-溴丙烯 → 4-Allyloxy-3-nitrobenzaldehyde

HRID 1176216

反应方程式

HRID 1176216 反应方程式
[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11].[CH2:13](Br)[CH:14]=[CH2:15]>>[CH2:15]([O:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11])[CH:14]=[CH2:13]

参与物

3

反应物 2

HCID 78413-溴丙烯HCID 181694-羟基-3-硝基苯甲醛

产物 1

HCID 224011524-Allyloxy-3-nitrobenzaldehyde

实验过程

Analogously to Method F, 25 g of 4-hydroxy-3-nitrobenzaldehyde and 25.1 ml of allyl bromide are reacted. The title compound is obtained as a slightly yellowish solid. Rf=0.30 (1:2 EtOAc-heptane). Rt=4.00.

来源与证据

ORD记录
ord-ee9a3375b8094033afe57a6e5cbb414d
来源数据集
uspto-grants-2010_11
专利号
US07842688B2

关联笔记

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