盐酸丁螺环酮 → 丁螺环酮

HRID 1402639

反应方程式

HRID 1402639 反应方程式
[CH:1]1[CH:2]=[N:3][C:4]([N:7]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][CH2:16][N:17]3[C:27](=[O:28])[CH2:26][C:21]4([CH2:25][CH2:24][CH2:23][CH2:22]4)[CH2:20][C:18]3=[O:19])[CH2:9][CH2:8]2)=[N:5][CH:6]=1.Cl>CCO>[CH:1]1[CH:6]=[N:5][C:4]([N:7]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][CH2:16][N:17]3[C:27](=[O:28])[CH2:26][C:21]4([CH2:22][CH2:23][CH2:24][CH2:25]4)[CH2:20][C:18]3=[O:19])[CH2:9][CH2:8]2)=[N:3][CH:2]=1

参与物

3

反应物 1

HCID 36431盐酸丁螺环酮

产物 1

HCID 2477丁螺环酮

试剂、催化剂与溶剂 1

HCID 702乙醇溶剂

实验过程

0.2 grams of Phospholipin 90 were dissolved in 2.5 grams EtOH; to this solution 0.02 grams of Vitamin E were added and mixed to obtain a clear system. To this system, 0.2 grams of buspirone HCl dissolved in 7.08 grams DDW were slowly added under constant stirring at room temperature in Heidolph mixer (700 rpm). The obtained system was stirred for additional 5 minutes.

后处理

  1. additionmixed
  2. customto obtain a clear system
  3. additionwere slowly added
  4. stirringThe obtained system was stirred for additional 5 minutes

来源与证据

ORD记录
ord-bf8638285ae54532a2da69bf1f4e4edb
来源数据集
uspto-grants-2014_12
专利号
US08911751B2

关联笔记

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