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4-叔丁基苄醇 → HCID 57118008，化合物
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 4-叔丁基苄醇 | HCID 13416 | — |
| 反应物 | 草酰氯 | HCID 65578 | — |
| 溶剂 | 乙醚 | HCID 3283 | — |
| 产物 | HCID 57118008 | HCID 57118008 | — |
反应步骤
To a stirred solution of oxalyl dichloride (100ml) in diethylether (500 ml) at -10° under nitrogen a solution of 4-t-butylbenzyl alcohol (200 ml) in diethylether (100 ml) was added dropwise so as to maintain the temperature between -10° and -5°. The solvent was then evaporated under vacuum to give the title compound (289 g,) as a clear oil (b.p. 120°-122° at 2 mbar).
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US05849907 |
| 来源数据集 | uspto-grants-1998_12 |
| ORD ID | ord-552cfa4c7d574c2cae876c5253dbc6fa |
| 来源说明 | uspto-grants-1998_12 |