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DL-酒石酸 → HCID 178418492,化合物
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | DL-酒石酸 | HCID 875 | — |
| 反应物 | 乙醚 | HCID 3283 | — |
| 反应物 | HCID 178418347 | HCID 178418347 | — |
| 溶剂 | 乙醇 | HCID 702 | — |
| 产物 | HCID 178418492 | HCID 178418492 | — |
反应步骤
First 0.15 g (0.001 mol) of anhydrous tartaric acid and then 0.39 g (0.001 mol) of trans-O-(4-chlorophenylacetyl)-4-(4-dimethylaminomethylphenyl)-cyclohexanol are dissolved in 7 ml of absolute ethanol. Diethyl ether is then added to the clear solution until it becomes slightly cloudy and it is then left to stand for 8 hours at +4° C. The crystalline product precipitated is suction filtered, washed with diethyl ether and dried.
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US05726205 |
| 来源数据集 | uspto-grants-1998_03 |
| ORD ID | ord-55aacc7a80b0419cab9d2c65fa6adadb |
| 来源说明 | uspto-grants-1998_03 |