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HRID 1663生成日期:2026年10月23日

DL-酒石酸 → HCID 178418492,化合物

https://huagongshe.com/zh-CN/reaction/1663

反应方程式

参与物

角色名称HCID投料
反应物DL-酒石酸HCID 875—
反应物乙醚HCID 3283—
反应物HCID 178418347HCID 178418347—
溶剂乙醇HCID 702—
产物HCID 178418492HCID 178418492—

反应步骤

First 0.15 g (0.001 mol) of anhydrous tartaric acid and then 0.39 g (0.001 mol) of trans-O-(4-chlorophenylacetyl)-4-(4-dimethylaminomethylphenyl)-cyclohexanol are dissolved in 7 ml of absolute ethanol. Diethyl ether is then added to the clear solution until it becomes slightly cloudy and it is then left to stand for 8 hours at +4° C. The crystalline product precipitated is suction filtered, washed with diethyl ether and dried.

来源与证据

DOI10.6084/m9.figshare.5104873.v1
专利号US05726205
来源数据集uspto-grants-1998_03
ORD IDord-55aacc7a80b0419cab9d2c65fa6adadb
来源说明uspto-grants-1998_03