3-甲基吲哚 → 4-Chloro-1-methyl-1H-indole

HRID 18284

反应方程式

HRID 18284 反应方程式
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][NH:6]2.[CH3:11]C1C2C(=CC=CC=2)NC=1>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][N:6]2[CH3:11]

参与物

3

反应物 2

HCID 67363-甲基吲哚HCID 913454-氯吲哚

产物 1

HCID 130487594-Chloro-1-methyl-1H-indole收率 100%

实验过程

According to the procedure of Preparation 13 (a), except substituting 4-chloroindole for the 3-methylindole, the title compound (2.2 g, 100%) was obtained as an amber oil: MS (ES) m/e 166.0 (M+H)+.

来源与证据

ORD记录
ord-9ecece90d71f49e38ad0702522d1c7ad
来源数据集
uspto-grants-2010_06
专利号
US07741339B2

关联笔记

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