丙酸钙 → Calcium propionate sorbate

HRID 2121069笔记

反应方程式

HRID 2121069 反应方程式
[C:1]([O-:5])(=[O:4])[CH2:2][CH3:3].[Ca+2:6].C([O-])(=O)CC.[C:12]([O-:19])(=[O:18])/[CH:13]=[CH:14]/[CH:15]=[CH:16]/[CH3:17].[K+]>O>[C:12]([O-:19])(=[O:18])/[CH:13]=[CH:14]/[CH:15]=[CH:16]/[CH3:17].[C:1]([O-:5])(=[O:4])[CH2:2][CH3:3].[Ca+2:6]

参与物

4

反应物 2

HCID 19999丙酸钙HCID 23676745山梨酸钾

产物 1

HCID 9964560Calcium propionate sorbate收率 90%

试剂、催化剂与溶剂 1

HCID 962聚[6-[4-(4-氰基苯基)苯氧基]己基甲基丙烯酸酯]溶剂2 次

实验过程

186 g (1 mol) of calcium propionate are dissolved in 500 ml of water. To this solution are added, at 25° C., a solution of 56 g (0.37 mol) of potassium sorbate in 60 ml of water. During addition a precipitate forms which is filtered off after 2 min. The precipitate is dried to constant weight at 150 mbar and 50° C. 90% pure calcium propionate sorbate is obtained as a white powder in 75% yield.

后处理

  1. additionTo this solution are added, at 25° C.
  2. additionDuring addition a precipitate forms which
  3. filtrationis filtered off after 2 min
  4. customThe precipitate is dried to constant weight at 150 mbar and 50° C

来源与证据

ORD记录
ord-d5a7903d4d7f4fe1b70509b8b6a822d5
来源数据集
uspto-grants-2004_02
专利号
US06693216B2

反应笔记

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