氯乙酰氯 → 4-(1-Methyl-1-cyclohexyloxycarbonyl)butyl methacrylate

HRID 225398

反应方程式

HRID 225398 反应方程式
C([C:3]1([OH:13])[CH:10]2[CH2:11]C3CC(CC1C3)[CH2:9]2)C.ClCC(Cl)=[O:17].[CH3:19][C:20]1([OH:26])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1.Cl[CH2:28][CH2:29][CH2:30][CH2:31][C:32](Cl)=[O:33]>>[C:3]([O:13][CH2:28][CH2:29][CH2:30][CH2:31][C:32]([O:26][C:20]1([CH3:19])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1)=[O:33])(=[O:17])[C:10]([CH3:11])=[CH2:9]

参与物

5

反应物 4

HCID 6577氯乙酰氯HCID 115501-甲基环己醇HCID 740895-氯代戊酰氯HCID 44019512-乙基-2-金刚烷醇

产物 1

HCID 689514664-(1-Methyl-1-cyclohexyloxycarbonyl)butyl methacrylate

实验过程

Synthetic experiment was conducted in the same manner as in Monomer Synthesis Example 1 except that 2-ethyl-2-adamantanol and chloroacetyl chloride were changed to 1-methyl-1-cyclohexanol and 5-chlorovaleryl chloride respectively, and the above described methacrylic derivative was obtained.

后处理

  1. customwas obtained

来源与证据

ORD记录
ord-ac9b16c39a5b4fdcb9182afcd0c3091f
来源数据集
uspto-grants-2009_07
专利号
US07556908B2

关联笔记

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