十六胺 → N-lauryl-N'-beta-chlorethylsulphonyl urea

HRID 26352

反应方程式

HRID 26352 反应方程式
[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:14]([NH2:30])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29].[Cl:31][CH2:32][CH2:33][S:34]([N:37]=[C:38]=[O:39])(=[O:36])=[O:35]>>[CH2:1]([NH:13][C:38]([NH:37][S:34]([CH2:33][CH2:32][Cl:31])(=[O:36])=[O:35])=[O:39])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:14]([NH:30][C:38]([NH:37][S:34]([CH2:33][CH2:32][Cl:31])(=[O:36])=[O:35])=[O:39])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

参与物

5

反应物 3

HCID 8926十六胺HCID 13583十二烷基伯胺HCID 785232-氯乙烷磺酰基异氰酸酯

产物 2

HCID 21322871N-lauryl-N'-beta-chlorethylsulphonyl ureaHCID 21322875N-hexadecyl-N'-beta-chlorethylsulphonyl urea

实验过程

Likewise it is possible to react 55.5 g (0.3 moles) of laurylamine or 72.3 g (0.3 moles) of hexadecylamine with 51.9 g (0.306 moles) of β-chlorethylsulphonyl isocyanate under the reaction conditions described to give N-lauryl-N'-β-chlorethylsulphonyl urea or N-hexadecyl-N'-β-chlorethylsulphonyl urea. N-lauryl-N'-β-chlorethylsulphonylurea:

后处理

  1. customunder the reaction conditions

来源与证据

ORD记录
ord-698b995e33214c32b6b25c60408de635
来源数据集
uspto-grants-1979_04
专利号
US04149979

关联笔记

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