Hydroxylamine → 苯甲羟肟酸

HRID 369477笔记

反应方程式

HRID 369477 反应方程式
[NH2:1][OH:2].C(=O)([O-])O.[Na+].[C:8](Cl)(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>C(OCC)(=O)C>[C:8]([NH:1][OH:2])(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

参与物

5

反应物 3

HCID 787HydroxylamineHCID 7412苯甲酰氯HCID 516892碳酸氢钠

产物 1

HCID 10313苯甲羟肟酸

试剂、催化剂与溶剂 1

HCID 8857乙酸乙酯溶剂

实验过程

To 156 mg of said compound (16) were added 2 ml of ethyl acetate, 2 ml of aqueous saturated sodium hydrogencarbonate, and 0.042 ml of benzoyl chloride and the mixture was reacted at room temperature for 3 hours to obtain a benzoylamino-alcohol compound (compound (17), C53H65NO14Si, molecular weight of 968.18).

后处理

  1. customthe mixture was reacted at room temperature for 3 hours

来源与证据

ORD记录
ord-16a1a81cf8bf4ff9a748fcb0588ba26e
来源数据集
uspto-grants-2000_10
专利号
US06136990

反应笔记

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