Hydroxylamine → 苯甲羟肟酸

HRID 369478笔记

反应方程式

HRID 369478 反应方程式
[NH2:1][OH:2].C(=O)([O-])O.[Na+].[C:8](Cl)(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>C(OCC)(=O)C>[C:8]([NH:1][OH:2])(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

参与物

5

反应物 3

HCID 787HydroxylamineHCID 7412苯甲酰氯HCID 516892碳酸氢钠

产物 1

HCID 10313苯甲羟肟酸

试剂、催化剂与溶剂 1

HCID 8857乙酸乙酯溶剂

实验过程

To 157 mg of said compound (19) were added 2 ml of ethyl acetate, 2 ml of aqueous saturated sodium hydrogencarbonate, and 0.012 ml of benzoyl chloride and the mixture was reacted at room temperature for 3 hours to obtain a benzoylamino-alcohol compound (compound (20), C53H65NO14Si, molecular weight of 968.18).

后处理

  1. customthe mixture was reacted at room temperature for 3 hours

来源与证据

ORD记录
ord-87ffac2d37474a9089950854203b8747
来源数据集
uspto-grants-2000_10
专利号
US06136990

反应笔记

加载中…