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碘甲烷 → 3-Hydroxy-2-iodo-1,6-dimethylpyridinium iodide
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 碘甲烷 | HCID 6328 | — |
| 反应物 | 3-羟基-2-碘-6-甲基吡啶 | HCID 89957 | — |
| 产物 | 3-Hydroxy-2-iodo-1,6-dimethylpyridinium iodide | HCID 22266466 | — |
反应步骤
2-Iodo-3-hydroxy-6-methylpyridine (835 mg) and iodomethane (3 mL) were added in glass sealed cube, and the reaction mixture was reacted at 130° C. for 4 h and at 180° C. for 1 h. The reaction mixture was completely evaporated to give 3-hydroxy-2-iodo-1,6-dimethylpyridinium iodide (2-014-02) (1.42 g).
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US08088924B2 |
| 来源数据集 | uspto-grants-2012_01 |
| ORD ID | ord-ac5bfb723490414b8bfa5d7705e7c0c2 |
| 来源说明 | uspto-grants-2012_01 |