糠醇 → 乙酸糠酯
反应方程式
[C:1]([O:4][C:5](=[O:7])[CH3:6])(=O)[CH3:2].C(O)C1[O:13][CH:12]=[CH:11][CH:10]=1>C(N(CC)CC)C>[C:5]([O:4][CH2:1][C:2]1[O:13][CH:12]=[CH:11][CH:10]=1)(=[O:7])[CH3:6]参与物
4
试剂、催化剂与溶剂 1
实验过程
Procedure was as in example 2, but acetic anhydride was added to the mixture of furfuryl alcohol and triethyl amine. The crude yield was 1149 g and the concentration was 58.7%, i.e., the yield was 99.5%. The crude product was washed 4 times with 200 ml water, whereby 641.3 g furfuryl acetate was obtained, its concentration was 96.2%, i.e., the yield was 91.0%.
后处理
- washThe crude product was washed 4 times with 200 ml water
来源与证据
- ORD记录
- ord-926e23620bc040f0978634dc078eb382
- 来源数据集
- uspto-grants-1977_02
- 专利号
- US04008256
反应笔记
加载中…