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2,4-二氯-6-硝基苯胺 → 10,12-Dichlorodibenzo[a,c]phenazine
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 2,4-二氯-6-硝基苯胺 | HCID 75893 | — |
| 反应物 | 1,2-Phenanthrenedione | HCID 3080566 | — |
| 溶剂 | 丙酮 | HCID 180 | — |
| 产物 | 10,12-Dichlorodibenzo[a,c]phenazine | HCID 21391728 | 81% |
反应步骤
When 0.12 mole each of 2,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 24 g. (81 percent yield) of 10,12-dichlorodibenzo[a,c]phenazine, mp = 221°-222° C. (acetone), were obtained.
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US04064127 |
| 来源数据集 | uspto-grants-1977_12 |
| ORD ID | ord-cf5c608cf4994a89b522be502c1d94b8 |
| 来源说明 | uspto-grants-1977_12 |