ethyl P-methyl-2-nitro-5-chlorophenylphosphinate → ethyl P-methyl-2-nitro-5-(2-pyridyloxy)phenylphosphinate

HRID 463559笔记

反应方程式

HRID 463559 反应方程式
[CH3:1][P:2]([C:7]1[CH:12]=[C:11](Cl)[CH:10]=[CH:9][C:8]=1[N+:14]([O-:16])=[O:15])(=[O:6])[O:3][CH2:4][CH3:5].[N:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[OH:23]>>[CH3:1][P:2]([C:7]1[CH:12]=[C:11]([O:23][C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][N:17]=2)[CH:10]=[CH:9][C:8]=1[N+:14]([O-:16])=[O:15])(=[O:6])[O:3][CH2:4][CH3:5]

参与物

3

反应物 2

HCID 53860251ethyl P-methyl-2-nitro-5-chlorophenylphosphinateHCID 178516071HCID 178516071，化合物

产物 1

HCID 54103496ethyl P-methyl-2-nitro-5-(2-pyridyloxy)phenylphosphinate

实验过程

Following the procedure of Example 17, ethyl P-methyl-2-nitro-5-chlorophenylphosphinate and 2-pyridyl alcohol are reacted together to give ethyl P-methyl-2-nitro-5-(2-pyridyloxy)phenylphosphinate.

后处理

  1. customare reacted together

来源与证据

ORD记录
ord-f92e8ec9354e47bd9589719a6231269b
来源数据集
uspto-grants-1985_05
专利号
US04520197

反应笔记

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