2-溴戊烷 → 2-Bromo-4-methylheptane

HRID 487516笔记

反应方程式

HRID 487516 反应方程式
[CH3:1][CH:2]([CH2:7][CH2:8][CH3:9])[CH2:3][CH:4](O)[CH3:5].P(Br)(Br)[Br:11].BrC(CCC)C>>[Br:11][CH:4]([CH2:3][CH:2]([CH3:1])[CH2:7][CH2:8][CH3:9])[CH3:5]

参与物

4

反应物 3

HCID 78902-溴戊烷HCID 24614三溴化磷HCID 1433454-METHYL-2-HEPTANOL

产物 1

HCID 153324532-Bromo-4-methylheptane

实验过程

17.50 g (0.135 mol) of 4-methylheptan-2-ol (3) was treated with PBr3 (13.48 g, 0.050 mol) as described above in the manufacture of 2-bromopentane (2). The product was purified by distillation at 165°-185° C. to yield 2-bromo-4methylheptane (4).

后处理

  1. distillationThe product was purified by distillation at 165°-185° C.

来源与证据

ORD记录
ord-e572b6fa4472487d82d0ff6de4893ed8
来源数据集
uspto-grants-1994_03
专利号
US05296220

反应笔记

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