化工社化工社化学信息打印报告 · 仅供科研参考
4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide → HCID 178418472，化合物
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide | HCID 53745902 | — |
| 反应物 | Sodium hydrogen sulphide | HCID 86586439 | — |
| 产物 | HCID 178418472 | HCID 178418472 | 63.6% |
反应步骤
Using the procedure in Preparation 34, 6.4 g (0.02 mol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide was reacted with 4.8 g (0.066 mol) of sodium hydrogen sulfide to afford 4.2 g of the title compound, mp 178°-180° C.
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US05620997 |
| 来源数据集 | uspto-grants-1997_04 |
| ORD ID | ord-10fcd818c14448c6a46b2fe2efcb38fe |
| 来源说明 | uspto-grants-1997_04 |