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HRID 752生成日期:2026年10月23日

对羟基苯甲酸 → Benzoic acid, 4-((1-oxodecyl)oxy)-

https://huagongshe.com/zh-CN/reaction/752

反应方程式

参与物

角色名称HCID投料
反应物对羟基苯甲酸HCID 135—
反应物吡啶HCID 1049—
反应物癸酰氯HCID 66982—
溶剂聚[6-[4-(4-氰基苯基)苯氧基]己基甲基丙烯酸酯]HCID 962—
产物Benzoic acid, 4-((1-oxodecyl)oxy)-HCID 3608562—

反应步骤

10 Grams of p-hydroxybenzoic acid and 15 g of decanoic acid chloride were stirred at room temperature, and 7.2 g of pyridine was dropwise added. After the mixture was stirred for 1 day, a reaction product was poured into water, and an organic layer was extracted with dichloromethane. The organic layer was washed with 1N hydrochloric acid and dried over anhydrous sodium sulfate, the solvent was distilled off, and then residue was washed with n-hexane and then dried to give a crude end product.

来源与证据

DOI10.6084/m9.figshare.5104873.v1
专利号US05723069
来源数据集uspto-grants-1998_03
ORD IDord-c218088b16c541088a933a7606f68c4c
来源说明uspto-grants-1998_03