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对羟基苯甲酸 → Benzoic acid, 4-((1-oxodecyl)oxy)-
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 对羟基苯甲酸 | HCID 135 | — |
| 反应物 | 吡啶 | HCID 1049 | — |
| 反应物 | 癸酰氯 | HCID 66982 | — |
| 溶剂 | 聚[6-[4-(4-氰基苯基)苯氧基]己基甲基丙烯酸酯] | HCID 962 | — |
| 产物 | Benzoic acid, 4-((1-oxodecyl)oxy)- | HCID 3608562 | — |
反应步骤
10 Grams of p-hydroxybenzoic acid and 15 g of decanoic acid chloride were stirred at room temperature, and 7.2 g of pyridine was dropwise added. After the mixture was stirred for 1 day, a reaction product was poured into water, and an organic layer was extracted with dichloromethane. The organic layer was washed with 1N hydrochloric acid and dried over anhydrous sodium sulfate, the solvent was distilled off, and then residue was washed with n-hexane and then dried to give a crude end product.
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US05723069 |
| 来源数据集 | uspto-grants-1998_03 |
| ORD ID | ord-c218088b16c541088a933a7606f68c4c |
| 来源说明 | uspto-grants-1998_03 |