Carbon Dioxide → 2-Methyl-1-naphthalenol propionate

HRID 1003125Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1003125
[CH3:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]=1[OH:12].COC(=O)[O-].[CH3:18][C:19]1C=CC2C(=CC=CC=2)[C:20]=1[OH:29].C1(O)C2C(=CC=CC=2)C=CC=1.FC(F)(F)C(OC1C=CC=CC=1)=O.C(=O)=O>>[C:20]([O:12][C:3]1[C:4]2[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=2)[CH:10]=[CH:11][C:2]=1[CH3:1])(=[O:29])[CH2:19][CH3:18]

Komponenten

6

Edukt 5

HCID 280Carbon DioxideHCID 70051-NaphtholHCID 240552-Methyl-1-naphthol3×HCID 68143Acetic acid, 2,2,2-trifluoro-, phenyl esterHCID 187952202-Methyl-1-naphthalenol methylcarbonate

Produkt 1

HCID 153947112-Methyl-1-naphthalenol propionate

Versuchsvorschrift

To demonstrate the storage stability of the compounds of the present invention, test samples of the title compounds of Examples 1, 2, 3, 4, 5 and 6 were placed in clear glass vials and kept on top of a laboratory desk for the time indicated. Samples of 2-methyl-1-naphthol, 1-naphthol and phenyl trifluoroacetate used as controls were similarly kept. One sample of 2-methyl-1-naphthol was stored under nitrogen and in a dry ice chest (temperature of approximately -50° C). A second sample of 2-methyl-1-naphthol and the remaining test'samples were stored at room temperature.

Aufarbeitung

  1. customwere stored at room temperature

Quellen und Nachweise

ORD-Eintrag
ord-72b9389a07ab4ed7a519daf6acf82b59
Quelldatensatz
uspto-grants-2000_04
Patentnummer
US06045590

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