HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Carbamate → 5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-ylmethyl 3,5-dichlorobenzoylcarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Carbamate | HCID 276 | — |
| Edukt | (5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-yl)methanol | HCID 473933 | — |
| Edukt | 3,5-Dichlorobenzoyl isocyanate | HCID 13513349 | — |
| Produkt | 5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-ylmethyl 3,5-dichlorobenzoylcarbamate | HCID 478191 | 78% |
Reaktionsschritte
The compound 19 (300 mg, 0.869 mmol) was converted to the carbamate with 3,5-dichlorobenzoyl isocyanate (1.5 eq.) in the same manner as the example 66 to give the compound 87 (380 mg, 78%) as crystals. Mp.124-125° C. Rf 0.23 (1:2 EtOAc-hexane)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06054591 |
| Quelldatensatz | uspto-grants-2000_04 |
| ORD ID | ord-c94c5db179054fd083e5aa12ed35038c |
| Quellennotiz | uspto-grants-2000_04 |