HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1008105Erstellt: 26. Oktober 2026
Trichloroacetonitrile → 3-{4-[2,4-bis(trichloromethyl)-s-triazine-6-yl]phenyl thio}propionic Acid
https://huagongshe.com/reaction/1008105
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Trichloroacetonitrile | HCID 11011 | — |
| Edukt | Aluminum bromide | HCID 24409 | — |
| Edukt | 3-[(4-Cyanophenyl)sulfanyl]propanoic acid | HCID 22666602 | — |
| Produkt | 3-{4-[2,4-bis(trichloromethyl)-s-triazine-6-yl]phenyl thio}propionic Acid | HCID 60111243 | — |
Reaktionsschritte
The reaction mixture of 22 g of 3-(4-cyanophenyl thio)propionic acid, 150 g of trichloroacetonitrile, and 2 g of AlBr3 was heated to 60° C. in order to dissolve the initially undissolved starting materials, and was bubbled by dry HCl at room temperature.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06797739B1 |
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| Quelldatensatz | uspto-grants-2004_09 |
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| ORD ID | ord-55159e626f014794ad064a59718bac78 |
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| Quellennotiz | uspto-grants-2004_09 |
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