反应详情

温度

60 °C

The reaction mixture of 22 g of 3-(4-cyanophenyl thio)propionic acid, 150 g of trichloroacetonitrile, and 2 g of AlBr3 was heated to 60° C. in order to dissolve the initially undissolved starting materials, and was bubbled by dry HCl at room temperature.

1. dissolutionto dissolve the
2. customwas bubbled by dry HCl at room temperature