1-Octanesulfonyl chloride → Octane-1-sulfonic acid [1-(4-amino-thieno[3,2-c]pyridin-2-ylmethyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-amide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	1-Octanesulfonyl chloride	HCID 82261	—
Edukt	N-[1-(4-Amino-thieno[3,2-c]pyridin-2-ylmethyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-4-(tetrahydropyran-4-yloxy)-benzenesulfonamide	HCID 22665795	—
Produkt	Octane-1-sulfonic acid [1-(4-amino-thieno[3,2-c]pyridin-2-ylmethyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-amide	HCID 86758421	—

Reaktionsschritte

This compound was prepared from 0.15 mL of octane sulfonyl chloride and 210 mg of 30a using the procedure described for 58c. Yield: 150 mg; m.p. 101-112° C., (+)-FAB-MS: 495 (MH+).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06797710B2
Quelldatensatz	uspto-grants-2004_09
ORD ID	ord-5a48b55f6cac4b2fb16c3a73a41544da
Quellennotiz	uspto-grants-2004_09