Ethyl Acetoacetate → Rac-2-acetyl-4-methoxy-3-oxo-butyric acid ethyl ester

HRID 1011950

Reaktionsgleichung

Reaktionsgleichung von HRID 1011950
[C:1]([O:7][CH2:8][CH3:9])(=[O:6])[CH2:2][C:3]([CH3:5])=[O:4].[CH3:10][O:11][CH2:12][C:13](Cl)=[O:14]>>[CH2:8]([O:7][C:1](=[O:6])[CH:2]([C:3](=[O:4])[CH3:5])[C:13](=[O:14])[CH2:12][O:11][CH3:10])[CH3:9]

Komponenten

3

Edukt 2

HCID 8868Ethyl AcetoacetateHCID 96623Methoxyacetyl chloride

Produkt 1

HCID 87352689Rac-2-acetyl-4-methoxy-3-oxo-butyric acid ethyl ester

Versuchsvorschrift

In analogy to the procedure described in Intermediate 11A], ethyl acetoacetate and methoxyacetylchloride gave the crude title compound in quantitative yield as yellow oil. MS: 202.9 (MH+).

Quellen und Nachweise

ORD-Eintrag
ord-525af10a5d2c4ad5b29c769a55edaab5
Quelldatensatz
uspto-grants-2011_07
Patentnummer
US07977358B2

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