HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl fluorosulfate → 3-(4-Methoxybenzylthio)-1-methylquinuclidinium fluorosulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl fluorosulfate | HCID 9870 | — |
| Edukt | 3-(4-Methoxybenzylthio)quinuclidine | HCID 19797265 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 3-(4-Methoxybenzylthio)-1-methylquinuclidinium fluorosulfonate | HCID 19797250 | — |
Reaktionsschritte
The procedure described in preparation 6-(3) was repeated, but using 756 mg of 3-(4-methoxybenzylthio) quinuclidine and 271 μl of methyl fluorosulfonate in the presence of 5 ml of methylene chloride, to afford 1.078 g of the title compound as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05104867 |
| Quelldatensatz | uspto-grants-1992_04 |
| ORD ID | ord-d6f53c977c6a4da88b5af247b46a3d95 |
| Quellennotiz | uspto-grants-1992_04 |