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HRID1030174

反应详情

EQUATION

反应方程式

HRID 1030174 的结构方程式

REACTANTS

反应物

2
结构：COS(=O)(=O)F
HCID9870

Fluorosulfuric acid, methyl ester

CH3FO3S

结构：COc1ccc(CSC2CN3CCC2CC3)cc1
HCID19797265

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(CSC2C[N+]3(C)CCC2CC3)cc1.O=S(=O)([O-])F
HCID19797250

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The procedure described in preparation 6-(3) was repeated, but using 756 mg of 3-(4-methoxybenzylthio) quinuclidine and 271 μl of methyl fluorosulfonate in the presence of 5 ml of methylene chloride, to afford 1.078 g of the title compound as an oil.

WORKUP

后处理

  1. customThe procedure described in preparation 6-(3)