Hydrochloric Acid → Benzoic Acid

HRID 1032866Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1032866
N(CCO)(CCO)CCO.Cl.[C:12]([O:20]C(=O)C1C=CC=CC=1)(=[O:19])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>OCC(CO)O.O>[C:12]([OH:20])(=[O:19])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 7167Benzoic anhydrideHCID 7618Triethanolamine

Produkt 1

HCID 243Benzoic Acid

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1533881,2,3-Propanetriol, mixt. with waterLösungsmittel

Versuchsvorschrift

Standard reaction conditions for the rate determinations in Table 1 are as follows: 60% glycerol/water (w/w), 120 ppm hardness (2:1 Ca:Mg), 10 mM Triethanolamine adjusted to pH 7 with HCl, and 50 umol benzoic anhydride. All incubations were at -10 deg. centigrade for 5 mins. Benzoic acid produced was measured by HPLC via an internal standard (acenaphthylene).

Aufarbeitung

  1. customStandard reaction conditions for the rate determinations in Table 1
  2. customwere at -10 deg.
  3. customfor 5 mins

Quellen und Nachweise

ORD-Eintrag
ord-3194e645c3e549f7846f0231da18903e
Quelldatensatz
uspto-grants-1994_05
Patentnummer
US05308529

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