HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl p-toluate → HCID 19023272, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl p-toluate | HCID 66743 | — |
| Edukt | N-bromobutanimide | HCID 67184 | — |
| Edukt | N-Cyclohexyl-N,4-dimethylbenzenesulfonamide | HCID 614169 | — |
| Produkt | HCID 19023272 | HCID 19023272 | 90,1% |
Reaktionsschritte
Utilising the procedure described in Example 1(a) employing N-cyclohexyl-N-methyl 4-methylbenzenesulphonamide (20.0 g, 0.075 mol) in lieu of ethyl 4-methylbenzoate and two equivalents of NBS (27.0 g, 0.15 mol) yielded a crude product of N-cyclohexyl-N-methyl 4-bromomethylbenzenesulphonamide (23.4 g, 90%) as an orange oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05314880 |
| Quelldatensatz | uspto-grants-1994_05 |
| ORD ID | ord-bdb763b948854923a02d346864ef977a |
| Quellennotiz | uspto-grants-1994_05 |