Pyridinium chloride → HCID 178457681, Verbindung
Reaktionsgleichung
[OH:1][C:2]([C:30]1[CH:35]=[CH:34][C:33]([C:36]2[N:41]=[C:40]([C:42]([NH:44][CH:45]([CH3:47])[CH3:46])=[O:43])[CH:39]=[CH:38][CH:37]=2)=[CH:32][CH:31]=1)([C:6]1[N:7]=[CH:8][N:9](C(C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)[CH:10]=1)[CH:3]([CH3:5])[CH3:4].Cl.N1C=CC=CC=1>>[OH:1][C:2]([C:30]1[CH:31]=[CH:32][C:33]([C:36]2[N:41]=[C:40]([C:42]([NH:44][CH:45]([CH3:47])[CH3:46])=[O:43])[CH:39]=[CH:38][CH:37]=2)=[CH:34][CH:35]=1)([C:6]1[N:7]=[CH:8][NH:9][CH:10]=1)[CH:3]([CH3:4])[CH3:5]Komponenten
3
Versuchsvorschrift
By the reaction in the same manner as in Example 4-(iii) using 6-{4-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl]phenyl}-N-isopropyl-2-pyridinecarboxamide (1.60 g) and pyridine hydrochloride (770 mg), the title compound (350 mg) was obtained as colorless powder crystals.
Aufarbeitung
- customBy the reaction in the same manner as in Example